The least inexpensive methylating reagent is Meerwein's salt. Me3OBF4. It's a solid so you should be able to handle it easily. Methyl triflate could be another option. Althohght many methylating electrophiles are available, their hard/soft properties need to match with that of your nucleophiles. |
使用硫酸二甲酯或者碘甲烷的时候在旁边准备点氨水,用过的仪器用氨水洗一下,反应完全后也应该向其中加入一些氨水处理过量的硫酸二甲酯或者碘甲烷,废液经氨水处理后再排放 |
提问时间: | 2024-11-03 |
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最近回答: | 2024-11-03 |